2-(10′,10′-Dimethyl-3′-sulfanylidene-4′-azatricyclo[5.2.1.01,5]decan-2′-yl)-10,10-dimethyl-4-azatricyclo[5.2.1.01,5]decane-3-thione
نویسندگان
چکیده
منابع مشابه
2-(10′,10′-Dimethyl-3′-sulfanylidene-4′-azatricyclo[5.2.1.01,5]decan-2′-yl)-10,10-dimethyl-4-azatricyclo[5.2.1.01,5]decane-3-thione
The title compound, C28H40N2O2S2, was obtained as a minor product from an anti-aldol reaction between the corresponding N-propionyl-thiol-actam and benzaldehyde. The asymmetric unit contains one half-molecule, which is completed by inversion symmetry. The molecule displays a nearly eclipsed conformation along the central C-C bond with a C-C-C-C- torsion angle of 20.4 (3)°.
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The title ionic compound, C16H36N(+)·C10H20B10N3O3(-), consists of a tetra-butyl-ammonium cation and a closo-deca-borate cluster anion, which is bound to the substituted 2,3-dihydro-1,2,4-oxadiazole ring through a B-N bond [1.540 (2) Å]. The distances between connected B atoms in the deca-borate cluster range from 1.689 (2) to 1.844 (2) Å. The 2,3-dihydro-1,2,4-oxadiazole ring adopts an envelop...
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ژورنال
عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online
سال: 2013
ISSN: 1600-5368
DOI: 10.1107/s1600536813019211